An Inert Atmosphere Glove Box for Organoboron Materials Chemistry

用于有机硼材料化学的惰性气氛手套箱

• 批准号: 472543-2015
• 负责人: Wang, Suning
• 金额: $ 4.09万
• 依托单位: Queen's University
• 依托单位国家: 加拿大
• 项目类别: Research Tools and Instruments - Category 1 (<$150,000)
• 财政年份: 2014
• 资助国家: 加拿大
• 起止时间: 2014-01-01 至 2015-12-31
• 项目状态: 已结题
• 来源: https://www.nserc-crsng.gc.ca/ase-oro/Details-Detailles_eng.asp?id=564781
• 关键词: Inert; Atmosphere; Glove; Box; Organoboron

An inert atmosphere glove box is a standard and indispensible equipment for research in inorganic and organometallic chemistry. The primary function of a dry box in our laboratory is for the storage/transferring of air and moisture sensitive compounds and the preparation of oxygen-free samples for the study of luminescence, photochromic switching and photoelimination properties of organoboron compounds and metal complexes. Because the photochemistry work requires a box that is free of halogenated solvent or reagents, our research requires two dedicated glove boxes, one for work that needs halogenated solvent/reagent free conditions and the other for all work that can tolerate or require the use of halogenated solvents or reagents.

惰性气氛手套箱是无机和有机金属化学研究中必不可少的标准设备。我们实验室干燥箱的主要功能是储存/转移对空气和湿气敏感的化合物，以及制备无氧样品，以研究有机硼化合物和金属配合物的发光、光致变色开关和光消除特性。由于光化学工作需要一个不含卤化溶剂或试剂的盒子，我们的研究需要两个专用手套箱，一个用于需要无卤化溶剂/试剂条件的工作，另一个用于所有可以耐受或需要使用卤化溶剂/试剂的工作溶剂或试剂。