MRI: Track 1 Acquisition of a Multifunctional Thermal Analysis Instrument for Interdisciplinary Research and Research Training in Advanced Nanomaterial Development

MRI：轨道 1 采购多功能热分析仪器，用于先进纳米材料开发的跨学科研究和研究培训

• 批准号: 2320284
• 负责人: Ellen Robertson
• 金额: $ 22.48万
• 依托单位: Union College
• 依托单位国家: 美国
• 项目类别: Standard Grant
• 财政年份: 2023
• 资助国家: 美国
• 起止时间: 2023-09-01 至 2026-08-31
• 项目状态: 未结题
• 来源: https://www.nsf.gov/awardsearch/showAward?AWD_ID=2320284&HistoricalAwards=false
• 关键词: MRI; Track; Acquisition; Multifunctional; Thermal

This award is jointly supported by the Major Research Instrumentation and the Chemistry Research Instrumentation programs. Union College is acquiring a thermogravimetric analyzer integrated with a Fourier Transform infrared spectrometer and a gas chromatograph/mass spectrometer (TGA/FTIR/GC/MS) system to support the research of Ellen Robertson, Ann Anderson, Mary Carroll, Yijing Stehle, and Christopher Whitehead and other colleagues at the institution. In general, a thermogravimetric analyzer (TGA) is a scientific instrument that aids the characterization of the structural, mechanical, chemical, and physical properties of materials as a function of temperature. However, having only information about the material weight loss as a function of temperature is not sufficient for answering the specific research questions associated with each material. Instead, a thorough characterization of the chemical species that are released during material heating is often desired. A TGA/FTIR/GC/MS system allows for the unambiguous identification of material thermal degradation products through the assignment of both vibrational modes (Fourier Transform Infrared Spectroscopy – FTIR) and molecular weight analysis (Mass Spectroscopy – MS). The instrument impacts many areas, such as chemistry, mechanical engineering, materials science, and nanotechnology. Furthermore, the new instrumen provides research and educational opportunities for a diverse group of at least 50 undergraduate students annually, both inside and outside of the classroom.The award is aimed at enhancing research and education at all levels. Research enabled by the instrument is focused on characterizing the structural, mechanical, chemical, and physical properties of diverse classes of modern nanomaterials, including plasmonic nanomaterials for detecting pollutants, semiconducting quantum dots for heavy metal sensing, metal oxide nanocrystals and aerogels for catalysis, and functionalized graphene oxide membranes for water filtration and purification. The instrument allows for the unambiguous identification of nanomaterial thermal degradation products through the assignment of both vibrational modes and molecular weight signatures.This award reflects NSF's statutory mission and has been deemed worthy of support through evaluation using the Foundation's intellectual merit and broader impacts review criteria.

该奖项由主要研究仪器和化学研究仪器项目共同支持，正在购买一台集成了傅里叶变换红外光谱仪和气相色谱/质谱仪（TGA/FTIR/GC/MS）系统的热重分析仪。 Ellen Robertson、Ann Anderson、Mary Carroll、Yijing Stehle 和 Christopher Whitehead 以及该机构其他同事的研究总体上是热重分析仪 (TGA)。是一种科学仪器，有助于表征材料的结构、机械、化学和物理特性随温度的变化。但是，仅获得有关材料失重随温度变化的信息不足以回答具体的研究。相反，通常需要对材料加热过程中释放的化学物质进行全面表征，以便通过分配两种振动来明确识别材料热降解产物。模式（傅里叶变换该仪器影响化学、机械工程、材料科学和纳米技术等许多领域。此外，该新仪器还为不同群体提供了研究和教育机会。每年至少有 50 名本科生在课堂内外学习。该奖项旨在加强各个级别的研究和教育，该仪器的研究重点是表征不同类别的结构、机械、化学和物理特性。现代的纳米材料，包括用于检测污染物的等离子体纳米材料、用于重金属传感的半导体量子点、用于催化的金属氧化物纳米晶体和气凝胶，以及用于水过滤和净化的功能化氧化石墨烯膜。该仪器可以通过纳米材料热降解产物的明确识别。振动模式和分子量特征的分配。该奖项反映了 NSF 的法定使命，并通过使用评估被认为值得支持基金会的智力价值和更广泛的影响审查标准。